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Biodegradable, superhydrophobic walnut wood membrane for the separation of oil/water mixtures

《化学科学与工程前沿（英文）》 2022年第16卷第9期页码 1377-1386 doi: 10.1007/s11705-022-2157-z

摘要： The preparation of environmentally friendly oil/water separation materials remains a great challenge. Freeze-drying of wood after lignin removal yields wood aerogels, which can be used as substrates to prepare fluorine-free environmentally friendly superhydrophobic materials, However, they are more suitable for absorption rather than filtration applications due to their poor strength. A study using cross-sections of pristine wood chips as substrates retains the original strength of wood, but the use of the cross-sectional of wood pieces limits their thickness, strength, and size. In this paper, a degradable fluorine-free superhydrophobic film (max. water contact angle of approximately 164.2°) with self-cleaning and abrasion resistance characteristics was prepared by a one-step method using pristine and activated walnut longitudinal section films as the substrate, with tetraethyl orthosilicate as a precursor and dodecyltriethoxysilane as a modifier. The tensile strength results show that superhydrophobic films with pristine or activated wood substrates maintained the strength of pristine wood and were 2.2 times stronger than the wood aerogel substrate. In addition, after cross-laminating the two samples, the films had the ability to separate oil and water by continuous filtration with high efficiency (98.5%) and flux (approximately 1.3 × 10³ L∙m^‒2∙h^‒1). The method has potential for the large-scale fabrication of degradable superhydrophobic filtration separation membranes.

关键词： wood nanotechnology superhydrophobic biodegradable surface modification oil/water separation

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超疏水SiO2/PS 薄膜于木材表面的构建

张明,王成毓

《中国工程科学》 2014年第16卷第4期页码 83-86

摘要：

通过溶胶-凝胶法一步合成疏水性且具备独特形貌的二氧化硅粒子，联合聚苯乙烯以滴涂的方式于木材表面仿生合成了稳定性超疏水薄膜。经处理后的木材表面与水的静态接触角为153°，滚动角小于5°。通过扫描电子显微镜照片观察到该复合涂层拥有微米/亚微米的二维等级粗糙结构，该结构协同低表面能物质共同决定超疏水性木材的成功制得。此外，进一步研究了超疏水性木材表面的稳定性和耐久性。结果表明，该超疏水性木材于水、腐蚀性液体（酸液/碱液）、常见有机溶剂中以及一些常见条件下仍保留超疏水特性，为未来木材材料的应用领域扩展提供了有利条件。

关键词：超疏水木材表面滴涂法复合薄膜

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一种提高超疏水木材机械稳定性的方法

王成毓,刘峰

《中国工程科学》 2014年第16卷第4期页码 79-82

摘要：

超疏水表面稳定性、耐久性的提升，对于其是否能达到商业应用的要求有着至关重要的作用。本文将聚乙烯醇（PVA）与二氧化硅（SiO₂）复合，通过滴涂法在木材表面形成一层有机-无机复合薄膜，之后对薄膜进行疏水改性，制得了一种机械稳健性较好的超疏水木材。所制得的木材有很好的防水性、较低的滚动角和较好的机械稳定性。

关键词：超疏水机械稳定性 PVA/SiO2 木材表面

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Bioinspired cellulose-based membranes in oily wastewater treatment

《环境科学与工程前沿（英文）》 2022年第16卷第7期 doi: 10.1007/s11783-021-1515-2

摘要：

• Cellulose-based membrane separates oily wastewater mimicking the living things.

关键词： Cellulose Bioinspired membrane Superhydrophobic surface Underwater superoleophobic surface Oil-water separation

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Effects of slip length and hydraulic diameter on hydraulic entrance length of microchannels with superhydrophobic

Wenchi GONG, Jun SHEN, Wei DAI, Zeng DENG, Xueqiang DONG, Maoqiong GONG

《能源前沿（英文）》 2020年第14卷第1期页码 127-138 doi: 10.1007/s11708-020-0661-8

摘要： This paper investigated effects of slip length and hydraulic diameter on the hydraulic entrance length of laminar flow in superhydrophobic microchannels. Numerical investigations were performed for square microchannels with Re ranging between 0.1 and 1000. It is found that superhydrophobic microchannels have a longer hydraulic entrance length than that of conventional ones by nearly 26.62% at a low Re. The dimensionless hydraulic entrance length slightly increases with the increasing slip length at approximately Re<10, and does not vary with the hydraulic diameter. A new correlation to predict the entrance length in square microchannels with different slip lengths was developed, which has a satisfying predictive performance with a mean absolute relative deviation of 5.69%. The results not only ascertain the flow characteristics of superhydrophobic microchannels, but also suggest that super hydrophobic microchannels have more significant advantages for heat transfer enhancement at a low Re.

关键词： laminar flow hydraulic entrance length super hydrophobic surface slip length hydraulic diameter

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Effective and selective separation of perrhenate from acidic wastewater by super-stable, superhydrophobic

《环境科学与工程前沿（英文）》 2022年第16卷第2期 doi: 10.1007/s11783-021-1456-9

摘要：

• A ZnO-biochar hybrid composite was prepared by solvothermal-pyrolysis synthesis.

关键词： Selectivity Adsorption Re(VII) ZnO Biochar

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Facile generation of highly durable thiol-functionalized polyhedral oligomeric silsesquioxane based superhydrophobic

《化学科学与工程前沿（英文）》 2022年第16卷第8期页码 1247-1258 doi: 10.1007/s11705-021-2124-0

摘要： In this study, a durable superhydrophobic/superoleophilic melamine foam was fabricated by a facile and rapid one-step thiol-ene click chemistry and Michael addition reaction, which demonstrated excellent robustness in oil/water separation. First, 1H, 1H, 2H-perfluoro-1-hexene reacted with thiol-functionalized polyhedral oligomeric silsesquioxane via the thiol-ene click chemistry to obtain a fluorinated thiol-functionalized polyhedral oligomeric silsesquioxane solution. Subsequently, the melamine foam was immersed to the solution system to form nanoaggregates on the melamine foam surface by the Michael addition reaction in the presence of ultraviolet light. The micro/nano rough structure and low surface energy of the nanoaggregates layer endowed the pristine melamine foam with superhydrophobicity; the water contact angle was greater than 150°. More importantly, the as-prepared melamine foam could withstand harsh conditions, such as a corrosive solution environment, strong ultraviolet light, mechanical compression, high and low temperature exposure, and ultrasonic washing. Driven by gravity, the as-prepared melamine foam could efficiently separate the oil/water mixtures and maintain 98% separation efficiency at high and low temperatures. In addition, it maintained the desirable absorption capability in different oil/organic solvents even after 15 absorption cycles. Accordingly, this facile, low-cost, and robust one-step method provides important support for the superhydrophobic oil/water separation field.

关键词： superhydrophobic melamine foam thiol-functionalized polyhedral oligomeric silsesquioxane durable oil/water separation

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溶胶-凝胶原位生长制备超疏水木材

梁金,吴义强,刘明

《中国工程科学》 2014年第16卷第4期页码 87-91

摘要：

采用溶胶-凝胶原位生长的方法制备超疏水木材，在木材表面形成一层纳米结构超疏水薄膜，水滴在木材表面接触角达到150.6°。采用X射线衍射仪（XRD）、扫描电子显微镜（SEM）、傅立叶变换红外光谱仪（FTIR）分别对超疏水木材样品的物相组成、表面形貌及表面化学官能团进行检测，分析表明木材的超疏水性是表面纳米级突起粗糙结构和乙烯基疏水基团共同作用的结果。

关键词：木材超疏水溶胶-凝胶纳米

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Preparation and properties of a silver particle-coated and 1-dodecanethiol-modified superhydrophobic

《化学科学与工程前沿（英文）》 2022年第16卷第8期页码 1237-1246 doi: 10.1007/s11705-022-2140-8

摘要： A Ag particle-coated and 1-dodecanethiol-modified melamine sponge (Ag-DDT-MS) was prepared through surface roughness by coating silver particles and subsequent grafting of a hydrophobic long hydrocarbon chain. Superhydrophobic and 3D porous Ag-DDT-MS was characterized by Fourier transform infrared spectroscopy, scanning electron microscope, energy-dispersive X-ray spectroscopy, and X-ray diffraction. The water contact angle of Ag-DDT-MS reached 159.2°. Ag-DDT-MS exhibited excellent absorption capacity for high viscous oils and organic solvents, ranging from 42.8 to 105.2 g∙g⁻¹. The absorbed oils can be easily collected by the mechanical pressing process, and the oil recovery rate was satisfactory, more than 90% after 20 recycles. Ag-DDT-MS material also demonstrated good stability and excellent compression-recovery ability, keeping 88.6% of the initial height after ten compression-release cycles.

关键词： melamine sponge oil-absorbing material hydrophobic oil-water separation oil absorption capacity

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A free-standing superhydrophobic film for highly efficient removal of water from turbine oil

Fan Shu, Meng Wang, Jinbo Pang, Ping Yu

《化学科学与工程前沿（英文）》 2019年第13卷第2期页码 393-399 doi: 10.1007/s11705-018-1754-3

摘要： A free-standing superhydrophobic film is prepared by sequentially dip-coating a commercially available filter paper with nano SiO suspension, epoxy emulsion, and octyltrimethoxysilane solution. A surface with micro- or nano-roughness is formed because SiO nanoparticles are uniformly and firmly adhered on the backbone of the filter paper by the cured epoxy resin. Furthermore, the surface energy is significantly reduced because of introducing octytrimethoxysilane. Such a surface structure makes the prepared film a superhydrophobic material. Due to its free-standing nature, this superhydrophobic film can be used to remove water from turbine oil by filtration. The efficiency of water removal is high (up to 94.1%), and the filtration process is driven solely by gravity without extra energy consumption. Because of the facile fabrication process and the high efficiency of water removal, this free-standing superhydrophobic film may find application in power industry.

关键词： superhydrophobicity nanoparticles dip coating epoxy emulsion turbine oil

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膜接触破乳——用于油包水乳液分离的超疏水ZIF-8@rGO膜 Article

顾佳慧, 瞿周, 张祥宁, 范红玮, 李春喜, Jürgen Caro, 孟洪

《工程（英文）》 2023年第23卷第4期页码 73-81 doi: 10.1016/j.eng.2022.02.017

摘要：

水-油界面不平衡是实现油包水乳液破乳的关键。传统膜通常是依赖较高的跨膜压力破坏界面平衡而实现破乳。本文提出了可自然、快速地破坏水-油界面平衡的“接触破乳”的概念，开发了一种对有机组分具有高通量的新型破乳分离膜。具体制备过程分为两步，首先通过真空辅助抽滤法在聚四氟乙烯（PTFE）基底上组装ZIF-8@rGO微球（ZGS）层，再采用聚二甲基硅氧烷（PDMS）交联溶液进行固定化处理。由于ZGS表面为微纳米阶层结构，所制备的ZIF-8@rGO@PDMS/PTFE（ZGPP）膜表面展现出超疏水性特性，当表面活性剂稳定的油包水乳液接触到膜表面时，微纳结构的超疏水膜表面会引起水-油界面不平衡。ZGPP膜对油包水乳液具有良好的分离破乳性能，在0.15 bar（15 kPa）的低跨膜压力下，分离效率可以达到99.57%，通量可达到2254 L·m^‒2·h^‒1，且对于表面活性剂稳定的纳米级甲苯水乳液（平均液滴尺寸为57 nm）的体系也可以实现破乳分离。“接触破乳”概念的提出有望为开发新一代油包水乳液分离的破乳膜提供新的思路。

关键词：油包水乳液破乳油水分离超疏水膜

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Cell surface protein engineering for high-performance whole-cell catalysts

Hajime Nakatani,Katsutoshi Hori

《化学科学与工程前沿（英文）》 2017年第11卷第1期页码 46-57 doi: 10.1007/s11705-017-1609-3

摘要： Cell surface protein engineering facilitated by accumulation of information on genome and protein structure involves heterologous production and modification of cell surface proteins using genetic engineering, and is important for the development of high-performance whole-cell catalysts. In this field, cell surface display is a major technology by exposing target proteins, such as enzymes, on the cell surface using a carrier protein. The target proteins are fused to the carrier proteins that transport and tether them to the cell surface, as well as to a secretion signal. This paper reviews cell surface display systems for prokaryotic and eukaryotic cells from the perspective of carrier proteins, which determine the number of displayed molecules, and the localization, size, and direction ( or terminal anchoring) of the passengers. We also discuss advanced methods for displaying multiple enzymes and a new method for the immobilization of whole-cell catalysts using adhesive surface proteins.

关键词： cell surface engineering surface display whole-cell catalysts bioprocess

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An Exploration of Surface Integrity Remanufacturing for Aeroengine Components

Qiao Xiang,Yong He,Ting-hong Hou

《工程管理前沿（英文）》 2016年第3卷第2期页码 107-114 doi: 10.15302/J-FEM-2016025

摘要： Surface integrity is the major factor impacting on the operation quality, service life and reliability of the aeroengine components. The surface integrity of aeroengine component is damaged by the failures such as crack, deformation, oxidation, corrosion, erosion, and microstructural degeneration. It adopts advanced remanufacturing technologies to restore or improve the surface integrity and regenerate these high value parts. This paper firstly puts forward the concept, namely surface integrity remanufacturing for aeroengine components, and its connotation. The key remanufacturing technologies have been developed to repair the components with surface damages. Ultimately, some application examples of surface integrity remanufacturing technologies as well as their effects in aeroengine maintenance are introduced. The discarded components have been reused and their service lives have been extended and their reliability has been increased by implementing surface integrity remanufacturing. It has realized “The Repaired Components Outpacing the New Ones”, material saving, energy saving, and emission reduction.

关键词： aeroengine component surface integrity remanufacturing surface integrity remanufacturing

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Review on mechanism and process of surface polishing using lasers

Arun KRISHNAN, Fengzhou FANG

《机械工程前沿（英文）》 2019年第14卷第3期页码 299-319 doi: 10.1007/s11465-019-0535-0

摘要： Laser polishing is a technology of smoothening the surface of various materials with highly intense laser beams. When these beams impact on the material surface to be polished, the surface starts to be melted due to the high temperature. The melted material is then relocated from the ‘peaks to valleys’ under the multidirectional action of surface tension. By varying the process parameters such as beam intensity, energy density, spot diameter, and feed rate, different rates of surface roughness can be achieved. High precision polishing of surfaces can be done using laser process. Currently, laser polishing has extended its applications from photonics to molds as well as bio-medical sectors. Conventional polishing techniques have many drawbacks such as less capability of polishing freeform surfaces, environmental pollution, long processing time, and health hazards for the operators. Laser polishing on the other hand eliminates all the mentioned drawbacks and comes as a promising technology that can be relied for smoothening of initial topography of the surfaces irrespective of the complexity of the surface. Majority of the researchers performed laser polishing on materials such as steel, titanium, and its alloys because of its low cost and reliability. This article gives a detailed overview of the laser polishing mechanism by explaining various process parameters briefly to get a better understanding about the entire polishing process. The advantages and applications are also explained clearly to have a good knowledge about the importance of laser polishing in the future.

关键词： laser polishing surface roughness process parameters mechanism

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Tribological study on the surface modification of metal-on-polymer bioimplants

《机械工程前沿（英文）》 2022年第17卷第2期 doi: 10.1007/s11465-022-0682-6

摘要： The tribological performance of artificial joints is regarded as the main factor of the lifespan of implanted prostheses. The relationship between surface roughness and coefficient of friction (COF) under dry and lubricated conditions is studied. Results show that under dry test, friction coefficient is not reduced all the time with a decrease in surface roughness. On the contrary, a threshold of roughness value is observed, and frictional force increases again below this value. This critical value lies between 40 and 100 nm in S_a (roughness). This phenomenon is due to the transfer of friction mechanisms from abrasion to adhesion. Under wet test, COF always decreases with reduction in surface roughness. This result is mainly attributed to the existence of a thin layer of lubricant film that prevents the intimate contact of two articulating surfaces, thus greatly alleviating adhesion friction. Furthermore, surface texturing technology is successful in improving the corresponding tribological performance by decreasing friction force and mitigating surface deterioration. The even-distribution mode of texturing patterns is most suitable for artificial joints. By obtaining the optimal surface roughness and applying texturing technology, the tribological performance of polymer-based bioimplants can be greatly enhanced.

关键词： artificial joints surface roughness friction surface texturing